by Nikolai V. Shokhirev
Prof. F. Ann Walker
Research Group,
Department of Chemistry,
University of Arizona,
Tucson, Arizona 85721, USA
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1D NMR Basics
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Introduction
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Bloch Equation
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Free Precession
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Numeric Experiments
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Fourier spectroscopy
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Continuous Wave Spectroscopy
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"Rotating" Frame
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Stationary Solution
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Saturation Effect
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Adiabatic Passage
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Multi-nuclei NMR spectra
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Pulse vs. CW Spectroscopy
2D NMR Basics
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Introduction
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Basic Pulse Scheme
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2D time domain spectrum
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2D frequency domain spectrum
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2D spectrum of interacting subsystems
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References
Chemical Exchange
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Chemical Reaction
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Modified Bloch Equation
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Two-site (isomer) reaction
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2D NMR with chemical exchange
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Rate constant extraction
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References
1D NMR with Chemical Exchange
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Continuous wave NMR spectrum
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Comparison of the 1D and 2D techniques
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Numerical modeling
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References
Programs
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Introduction
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Program "Bloch"
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Programs "TwoLines1D" and "TwoLineNMR"
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Program "TwoSiteExchange"
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